Heidolph Synthesis 1 Mode D'emploi page 57

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4.1
Reaction vessels ................................................................................. 80
4.2
Locate reaction vessels in heater block .............................................. 80
4.3
Connect vacuum ................................................................................. 81
4.4
4.4.1
Set-up stand........................................................................................ 82
4.4.2
Install cooler ........................................................................................ 82
4.4.3
Connect vacuum and coolant.............................................................. 83
4.4.4
Install receiving flask ........................................................................... 83
4.5
4.6
Schematic, Multi-Evaporator with vacuum control............................... 84
5.
Electric wiring................................................................................................. 86
6.
Install guard hood .......................................................................................... 86
6.1
Guard hood ......................................................................................... 86
6.2
Installation ........................................................................................... 87
7.
Exchange reaction blocks .............................................................................. 87
OPERATION ............................................................................................................ 89
8.
General .......................................................................................................... 89
9.
Controls, brief description .............................................................................. 89
9.1
Power switch ....................................................................................... 89
9.2
Start / Stop shaking action .................................................................. 89
9.3
Start / Stop heater ............................................................................... 90
9.4
Set / edit parameters........................................................................... 90
9.5
Set or display ...................................................................................... 90
9.6
Select value......................................................................................... 90
9.7
Set temperature gradient .................................................................... 90
9.8
Activate temperature gradients ........................................................... 90
9.9
Identic ................................................................................................. 90
10.
Setting work in detail...................................................................................... 91
10.1
Set shaking frequency......................................................................... 91
10.2
10.2.1 Setting ................................................................................................. 91
10.2.2 Temperature setting, limiting values.................................................... 91
10.3
10.4
Set timer.............................................................................................. 91
10.5
Set temperature gradient .................................................................... 92
10.5.1 Set values ........................................................................................... 92
10.5.2 Delete values ...................................................................................... 93
10.5.3 Limiting temperatures.......................................................................... 93
10.6
Activate temperature gradient ............................................................. 93
10.7
Turn shaking action ON ...................................................................... 94
10.8
Turn heater ON ................................................................................... 94
11.
External temperature sensor.......................................................................... 94
11.1
Temperatures below solvent's boil point ............................................. 95
11.2
Temperatures above solvent's boil point. ............................................ 95
11.3
In the use as multi evaporator ............................................................. 95
12.
Setup (timer and temperature sensor) ........................................................... 96
13.
Filter action, solid-phase synthesis ................................................................ 97
14.
Use condensation zone ................................................................................. 98
15.
16.
Access to rear reaction vessels ..................................................................... 99
17.
Interface RS 232 .......................................................................................... 100
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