Tintometer Lovibond MD100 Mode D'emploi page 39

Methods
GB
Notes:
1. Vial cleaning:
As many household cleaners (e.g. dishwasher detergent) contain reducing substances,
the subsequent determination of Chlorine may show lower results. To avoid any meas-
urement errors, only use glassware free of Chlorine demand.
Preparation: Put all applicable glassware into Sodium hypochlorite solution (0.1 g/l) for
one hour, then rinse all glassware thoroughly with deionised water.
2. For individual testing of free and total Chlorine, the use of different sets of glassware is
recommended (EN ISO 7393-2, 5.3)
3. Preparing the sample:
When preparing the sample, the lost of Chlorine, e.g. by pipetting or shaking, must be
avoided. The analysis must take place immediately after taking the sample.
4. The DPD colour development is carried out at a pH value of 6.2 to 6.5. The reagents
therefore contain a buffer for the pH adjustment.
Strong alkaline or acidic water samples must be adjusted between pH 6 and pH 7 before
the reagent is added (use 0.5 mol/l Sulfuric acid resp. 1 mol/l Sodium hydroxide).
5. Exceeding the measuring range:
Concentrations above 4 mg/l Chlorine using liquid reagents can lead to results showing
0 mg/l. In this case, the water sample must be diluted with water free of Chlorine and
the measurement repeated.
6. After using liquid reagents replace the bottle caps securely noting the colour coding.
Store the reagent bottles in a cool, dry place ideally between 6°C and 10°C.
7. Oxidising agents such as Bromine, Ozone etc. interfere as they react in the same way as
Chlorine.
8. In samples with high Calcium ion contents* and/or high conductivity* can lead to turbid-
ity of the sample and therefore incorrect measurements. In this case, the reagent tablets
DPD No. 1 High Calcium and DPD No. 3 High Calcium should be used as an alternative.
(Order-No.: see reagents „Chlorine with Tablet").
* it is not possible to give exact values, because the development of turbidity depends
on the nature of the sample.
Reagent
Set
DPD No. 1 buffer solution
DPD No. 1 reagent solution
DPD No. 3 solution
DPD No. 1 buffer solution
DPD No. 1 reagent solution
DPD No. 3 solution
MD100_10 12/2016
Form of reagent/Quantity
(approx. 300 tests)
3 x Liquid reagent / 15 ml
1 x Liquid reagent / 15 ml
2 x Liquid reagent / 15 ml
Liquid reagent / 15 ml
Liquid reagent / 15 ml
Liquid reagent / 15 ml
Order-No.
471056
471010
471020
471030
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